低腐蚀耐高温高密度无固相完井液技术研究

Research on Low-Corrosive, High Temperature-Resistant, High-Density, and Solid-Free Completion Fluid

  • 摘要: 针对南海某高温高压井极端工况对完井液耐高温、高密度、低腐蚀速率和储层保护等性能的要求,通过优化高价金属盐离子配比来调控溶液结晶点与密度梯度,构建了耐高温高密度无固相完井液体系。采用高温老化试验、腐蚀测试和渗透率恢复测试等方法,测试了完井液的密度稳定性、天然气水合物抑制性、腐蚀速率和储层保护性等关键性能。结果表明:高密度无固相完井液密度可达1.85 kg/L,在170 ℃温度下老化3 d后密度波动仅为0.01 kg/L;具有良好的天然气水合物抑制性能,结晶温度≤−12.5 ℃;高温高压条件下完井液密度变化率仅为3.8%;腐蚀速率低于0.076 mm/a,满足行业指标要求;平均岩心渗透率恢复率达87.94 %。现场应用验证了无固相完井液在控制水锁效应、有效抑制天然气水合物生成、维持井筒完整性方面的有效性,投产后增产效果好,实际产气量是配产气量的133 %。无固相完井液为高温高压油气田完井作业提供了新的技术途径。

     

    Abstract: In order to meet the requirements of properties including high temperature resistance, high density, low corrosion rate, and reservoir protection, etc. for completion fluids under harsh working conditions in a high-temperature and high-pressure well in the South China Sea, the ratio of high valency metal salt ions was optimized to regulate the crystallization point and density gradient of the solution, and a high temperature-resistant, high-density, and solid-free completion fluid system was constructed. Through methods such as high-temperature aging experiments, corrosion testing, and permeability recovery testing, the key properties of the completion fluid, such as density stability, hydrate inhibition, corrosion rate, and reservoir protection, were tested. The results show that the density of the high-density and solid-free completion fluid can reach up to 1.85 kg/L. After aging at a temperature of 170 °C for 3 days, the density fluctuation was only 0.01 kg/L, indicating good natural gas hydrate inhibition performance and a crystallization temperature of less than −12.5 °C. The density change rate of the completion fluid under high-temperature and high-pressure conditions was only 3.8%. The corrosion rate was less than 0.076 mm/a, meeting the industry standard requirements. The average core permeability recovery value reached 87.94%. The field application has verified the effectiveness of the solid-free completion fluid in controlling the water lock effect, hydrate inhibition, and maintaining wellbore integrity. After the application of the completion fluid, positive production increase response was observed, and the actual gas production rate reached 133% of the design capacity. This solid-free completion fluid provides a new technical solution for high-temperature and high-pressure oil and gas field completion operations.

     

/

返回文章
返回