新疆风城油田稠油热采高温封堵剂研究与现场试验

Study and Field Test on a High Temperature Plugging Agent for the Thermal Recovery of Heavy Oil in Fengcheng Oilfield, Xinjiang

  • 摘要: 新疆风城油田稠油热采过程中容易发生蒸汽地下窜流和地表汽窜,严重影响产能水平,还会造成地面污染。针对这些问题,开展了稠油热采高温封堵剂研究。以苯酚、甲醛为主要原料,有机胺为催化剂,合成了油溶性酚醛树脂OSR,并与环氧树脂、有机硅偶联剂、稀释剂等复配,研制了新型酚醛环氧树脂类高温封堵剂HTD。在实验室模拟稠油油藏条件,将HTD与一定粒径的石英砂混合充填、压实、高温养护,进行了高温成胶固化试验,评价了高温固化性能、耐温性能及高温封堵性能等,并在3口井进行了现场试验。室内试验得出,HTD的抗温能力可达300 ℃以上,在温度高于180 ℃时与石英砂固结体的抗压强度高于12 MPa,在220~300 ℃条件下对高渗透率岩心的封堵率高于99.5%,突破压力梯度大于35 MPa/m;现场试验后,封堵了蒸汽窜流通道,试验区恢复了正常蒸汽吞吐生产,注汽压力3.5~5.5 MPa,试验两年后,产油水平提升至62.12 t/d,平均日增油22.7 t,取得了良好的经济效益。研究结果表明,HTD具有优良的耐温性能和封堵性能,可有效封堵蒸汽地下窜流和地表汽窜通道,增大蒸汽波及体积,提高油井产能,且有效期长,具有很好的应用价值。

     

    Abstract: Underground and surface steam channeling were easily encountered during thermal recovery of heavy oil in Fengcheng Oilfield, Xinjiang, and it seriously affected the productivity level and caused surface pollution. To solve this problem, research on a high temperature plugging agent for thermal recovery of heavy oil was carried out. Oil soluble phenolic resin OSR was synthesized with phenol and formaldehyde as main raw materials and organic amine as catalyst. A new phenolic epoxy resin type of high temperature plugging agent, HTD, was developed with epoxy resin, organic silicone coupling agent and diluents. Under simulated heavy oil reservoir conditions in the laboratory, HTD was mixed with quartz sand in certain particle size for filling, compaction and high-temperature maintenance. In addition, high-temperature gelling and curing experiments were conducted. Temperature resistance, and high temperature curing performance and plugging effect were evaluated followed by field tests on three wells. The experimental results showed that HTD could resist high temperature over 300 ℃ and its compressive strength was greater than 12 MPa when combined with quartz sand at a temperature above 180 ℃. The plugging rate of high permeability core was greater than 99.5% at 220–300 ℃ with a breakthrough pressure gradient over 35 MPa/m. In field tests, steam channeling was blocked and production by steam huff and puff came back to normal with the pressure of 3.5–5.5 MPa. Two years later, oil production rose to 62.12 t/d with an average daily increase of 22.7 t, achieving sound economic benefits. Research results show that HTD has excellent temperature resistance and plugging performance and can effectively block surface and underground steam channeling. HTD has a good application value, for it can expand steam sweep volume and improve oil well productivity, showing a long validity period.

     

/

返回文章
返回